第一部分 分析化学实验基本知识 1
第二部分 基础实验 5
实验一 滴定分析基本操作 5
Experiment 1 The Basic Operation in TitrimetricAnalysis 9
实验二 电子天平与称量练习 14
Experiment 2 Electronic Analytical Balance and Weighing Exercise 16
实验三0.1 mol/LHCl标准溶液的配制和标定 18
Experiment 3 Preparation and Standardization of Standard 0.1 mol/L Hydrochloric Acid Solution 20
实验四 混合碱的含量测定 22
Experiment 4 Determination ofMixed Base 24
实验五0.1 mol/L氢氧化钠标准溶液的配制与标定 26
Experiment 5 Preparation and Standardization of Standard Solution of 0.1 mol/L SodiumHydroxide Solution 28
实验六阿司匹林的含量测定 30
Experiment 6 Determination ofAspirin 32
实验七0.05 mol/LEDTA标准溶液的配制与标定 34
Experiment 7 Preparation and Standardization of 0.05 mol/L EDTA Standard Solution 36
实验八EDTA对铅、铋混合溶液的连续滴定 38
Experiment 8 Continuous Titration ofPb2+and Bi3+Mixed Solution by EDTA 40
实验九EDTA标准溶液的标定及自来水总硬度的测定 42
Experiment 9 EDTA Solution Calibration and Determination of Tap Water Hardness 44
实验十0.1 mol/LNa2S2O3标准溶液的配制和标定 46
Experiment 10 Preparation and Standardization of 0.1 mol/L Sodium Thiosulfate Standard Solution 48
实验十一碘量法测定维生素C的含量 51
Experiment 11 VitaminCDeterminationbyIodineTitration 53
实验十二碘量法测定葡萄糖的含量 55
Experiment 12 Determination ofGlucose by Iodimetry 57
实验十三0.02 mol/L高锰酸钾标准溶液的配制与标定 59
Experiment 13 Preparation and Standardization of 0.02 mol/L Standard Potassium Permanganate Solution 61
实验十四过氧化氢的含量测定 63
Experiment 14 Determination ofHydrogen Peroxide 65
实验十五硝酸银标准溶液的配制和标定 67
Experiment 15 Preparationand Standardizationofthe StandardSilverNitrateSolutions 69
实验十六氯化铵的含量测定 72
Expenment 16 Determination ofAmmoniumChloride 74
实验十七 自来水中氯含量的测定 76
Experiment 17 TheDeterminationoftheContentofChlorineinTapWater 78
实验十八氯化钡中结晶水测定 80
Experiment 18 Determination of Water in Barium Chloride Dihydrate 82
实验十九磷酸的电位滴定 84
Experiment 19 The Potentiometric Titration of Phosphoric Acid 86
实验二十用氟离子选择电极测定水中氟离子含量 88
Experiment 20 Determination of F-in Water by Fluorine Ion-Selective Electrode 90
实验二十一永停滴定法标定I2标准溶液 93
Experiment 21 Standardization of I2Standard Solution by Dead-stop Titration Method 95
实验二十二紫外-可见分光光度法测定维生素B12注射液的含量 97
Experiment 22 Determination of Vitamin B 12 Injection by UV Spectrophotometry 99
实验二十三比色法测定芦丁的含量 101
Experiment 23 Determination ofthe Content ofRutin by Colorimetry 103
实验二十四荧光分光光度法测定维生素B2的含量 105
Experiment 24 Determination ofVitamin B2 by Fluorescence Spectrometry 107
实验二十五苯和二甲苯气相色谱实验条件的考察 109
Experiment 25 Experimental Conditions Study for Benzene and Methylbenzene AnalyzedbyGas Chromatography 111
实验二十六HPLC法测定感冒胶囊中咖啡因的含量 114
Experiment 26 Determination ofCaffeine in Ganmao Capsule by HPLC 116
实验二十七水杨酸红外光谱的测定 118
Experiment 27 Determination of Salicylic Acid Chemical Structure by IR Spectrophotometry 120
实验二十八薄层色谱的制备和应用 122
Experiment28 Preparation andApplicationofThinLayerChromatography 124
第三部分 设计性实验 127
实验二十九食醋总酸度的测定 127
Experiment29 Determination ofTotalAcidityofVinegar 128
实验三十蛋壳中钙、镁的含量测定 129
Experiment 30 Determination of Calcium and Magnesium Content in Eggshell 130
第四部分 大型分析仪器仿真操作 132
实验三十一气相色谱-质谱联用仪的仿真操作 132
Experiment 31 Gas ChromatographyMass Spectrometry (GC-MS) 134
实验三十二红外光谱仪仿真操作 136
Experiment 32 Infrared Spectroscopy(IR) 137
实验三十三原子吸收分光光度计的仿真操作 139
Experiment 33 Atomic Absorption Spectrophotometer(AAS) 142
实验三十四高效液相色谱的仿真操作 146
Experiment 34 HighPerformanceLiquidChromatography(HPLC) 147
第五部分 附录 149
附录1常用指示剂 149
附录2常用缓冲溶液的配制 152
附录3 0~95 ℃时标准缓冲溶液的pH 153
附录4常用酸碱的密度、含量和浓度 154
参考文献 155