第一章 中成药分析实验的基本知识 1
Chapter One Elementary Knowledge of Experiment for Analysis of Traditional Chinese Patent Medicine 1
第一节 中成药分析实验基本要求及注意事项 1
Section Ⅰ Basic Requirements and Announcements of Traditional Chinese Patent Medicine Analysis Experiment 2
第二节 供试品溶液的制备方法 4
Section Ⅱ Preparation of Test Solution 6
第三节 中成药分析实验中常用的分析方法 9
Section Ⅲ Commonly Used Analytical Methods for Experiment of Traditional Chinese Patent Medicine 16
第四节 分析方法学的基本内容 24
Section Ⅳ The Basic Content of Analysis Method 27
第二章 中成药分析实验 30
Chapter Two Experiment for Analysis of Traditional Chinese Patent Medicine 30
实验一 五苓散和万氏牛黄清心丸的显微鉴别 30
1．Microscopical Identification of Wuling Powder and Wanshi Niuhuang Qingxin Pills 33
实验二 安胃片与冰硼散的理化鉴别 37
2．Physical-Chemical Identification of Anwei Tablets and Bingpeng Powder 40
实验三 桂枝茯苓丸与葛根芩连片的薄层色谱鉴别 43
3．Identification of Guizhi Fuling Pills and Gegen Qinlian Tablets by TLC 47
实验四 附子理中丸中乌头碱及砷盐的限量检查 52
4．Limit Test of Aconitine and Arsenate in Fuzi Lizhong Pills 55
实验五 甲苯法测定通宣理肺丸中的水分 59
5．Determination of Water in Tongxuan Lifei Pills 61
实验六 气相色谱法测定藿香正气水中乙醇的含量 64
6．Determination of Ethanol in Huoxiang Zhengqi Tincture by GC 66
实验七 黄连上清丸中重金属的检查 69
7．Test of Heavy Metals in Huanglian Shangqing Pills 72
实验八 酸性染料比色法测定华山参片总生物碱的含量 75
8．Determination of the Total Alkaloids in Tabellae Physochlainae by Acid-dye Colorimetry 77
实验九 柱色谱-紫外分光光度法测定戊己丸中总生物碱的含量 80
9．Determination of the Total Alkaloids in Wuji Pills by Column Chromatography-UV Spectrophotometry 82
实验十 气相色谱法测定西瓜霜润喉片中冰片的含量 84
10．Determination of Borneolum Syntheticum in Xiguashuang Runhou Tablets by GC 86
实验十一 HPLC法测定逍遥丸中芍药苷的含量 89
11．Determination of Paeoniflorin in Xiaoyao Pills by HPLC 91
实验十二 HPLC法测定银杏叶片中总黄酮醇苷的含量 93
12．Determination of Total Amount of Flavonol Glycosides in Yinxingye Tablets by HPLC 95
实验十三 二妙丸的鉴别与挥发油的测定 98
13．Identification of Ermiao Pills and Determination of Volatile Oil 101
实验十四 大山楂丸的鉴别及总黄酮的含量测定 104
14．Identification of Dashanzha Pills and Determination of Total Flavonoids 108
实验十五 注射用双黄连（冻干）的质量分析 112
15．Quality Analysis of Shuanghuanglian Injection 117
实验十六 牛黄解毒片的理化鉴别及羟基蒽醌的含量测定 124
16．Physical-Chemical Identification of Niuhuan Jiedu Tablets and Determination of Hydroxyanthraquinone 128
实验十七 六味地黄丸的质量分析 132
17．Quality Analysis of Liuwei Dihuang Pills 136
实验十八 设计安神补脑液的质量分析方法 142
18．Design the Analysis Experiment for Anshen Bunao Mixture 144
实验十九 设计止喘灵注射液的质量分析方法 146
19．Design the Analysis Experiment for Zhichuanling Injection 147
实验二十 设计复方丹参片的质量分析方法 149
20．Design the Analysis Experiment for Compound Salvia Tablets 150
附录 152
Appendix 152
一、常用薄层色谱显色剂的配制和使用 152
1．The Preparation and Usage of Commonly Used TLC colorant 155
二、中国药典收载的对照品 158
2．Chemical Reference Substance listed in Chinese Pharmacopoeia 158