Experiment 1 Preparation of Aspirin 1
Introduction 1
Experiment 2 Preparation of Paracetamol 8
Introduction 8
Experiment 3 Preparation of Benorylate 13
Introduction 13
Experiment 4 Preparation of Chlorobutanoium 18
Introduction 18
Experiment 5 Preparation of Nikethamide 20
Introduction 20
Experiment 6 Stability Study of Procaine Hydrochloride 24
Introduction 24
Experiment 7 Preparation of Biphenyl Ketobutyric Acid 28
Introduction 28
Experiment 8 Simple Distillation 33
Experiment 9 Melting Point Determination 35
Experiment 10 Recristallization 39
Experiment 11 Determination of Optical Rotation 42
the Laboratoty Report of Medicinal Chemistry 47
实验一 阿司匹林的制备 49
实验二 扑热息痛的制备 52
实验三 苯乐来的制备 54
实验四 三氯叔丁醇的制备 57
实验五 尼克刹米的制备 59
实验六 盐酸普鲁卡因的稳定性 61
实验七 联苯丁酮酸的制备 63
实验八 简单蒸馏 65
实验九 熔点测定 68
实验十 重结晶 70
实验十一 旋光度的测定 74
实验报告格式 78
Annex（附录） 79