第一篇 基础化学实验基本知识 1
第一章 绪论 1
第二章 化学实验常用的仪器 9
第三章 化学实验中的数据表达与处理 22
第二篇 基础化学实验课题 25
实验一 常用容量分析玻璃仪器的操作练习 25
实验二 分析天平称量练习 33
实验三 缓冲溶液的配制和性质、溶液pH值测定 38
实验四 氯化钠的精制 42
实验五 硫酸亚铁铵的制备 45
实验六 标准溶液的配制与标定 48
实验七 返滴定法测定阿司匹林的含量 56
实验八 双氧水中过氧化氢含量的测定 59
实验九 碘量法测定维生素C的含量 61
实验十 水硬度测定 64
实验十一 硫氰酸盐可见分光光度法测定水样中铁含量 68
实验十二 置换法测定镁的原子量 72
实验十三 凝固点降低法测定葡萄糖相对分子量 75
实验十四 化学反应速率与活化能的测定 78
实验十五 分光光度法测定磺基水杨酸合铁（Ⅲ）的组成和稳定常数 82
实验十六 葡萄糖酸锌的制备与含量测定 85
实验十七 醋酸解离平衡常数、电离度的测定及食醋中HAc含量的测定 88
实验十八 绿茶、红茶、黑茶和半发酵茶中钙、镁和微量元素铁的综合测定 91
实验十九 环境水样无机化学性质评价 96
实验二十四 苯基卟啉及其金属化合物的合成 101
实验二十一 实验设计与研究 104
Part Ⅰ Experiment Essentials in General Chemistry 107
Chapter 1 Introduction 107
Chapter 2 Ordinary Instruments in Chemical Experiments 117
Chapter 3 Evaluation of Analytical Results 130
Part Ⅱ Experiment in General Chemistry 135
Experiment 1 Operation of Volumetric Analysis 135
Experiment 2 Weighing Practice of Analytical Balance 145
Experiment 3 Preparation and Properties of Buffers and Measure the pH of the Solution 151
Experiment 4 Refining Sodium Chloride 156
Experiment 5 Preparation of Ammonium Iron(Ⅱ)Sulfate 160
Experiment 6 Preparation and Standardization of Standard Solution 164
Experiment 7 The Determination of the Aspirin Content by the Back Titration Method 175
Experiment 8 Determination of the Concentration of Commercial Hydrogen Peroxide by Potassium Permanganate Method 178
Experiment 9 Determination of Vitamin C by an Iodometric Titration 181
Experiment 10 Determination of the Hardness of Water by Complexometric Titration 184
Experiment 11 To Determine the Fe3+ Concentration of Water with Spectrophotometric Method 189
Experiment 12 Determination of the Atomic Mass of Mg by Displacement Method 193
Experiment 13 Molar Mass of Glucose by Freezing Point Depression 197
Experiment 14 Determination of the Chemical Reaction Rate and Activation Energy 200
Experiment 15 Determination of the Composition and the Stability Constant of 5-sulfosalicylate iron(Ⅲ)Complex by Spectrophotometry 205
Experiment 16 Preparation and Content Determination of Zinc Gluconate 209
Experiment 17 Determination of Dissociation Equilibrium Constant of Acetic Acid and Determination of the Percentage of Acetic Acid in Vinegar 213
Experiment 18 Comprehensive Determination of Calcium,Magnesium and Trace Element Iron in Green,Red,Black and Half-fermented Tea 217
Experiment 19 Inorganic Chemistry Analysis of Environmental Water Samples 223
Experiment 20 The Synthesis of Tetraphenylporphine and Metalloporphyrin Complexes 229
Experiment 21 Experiment Design and Research 233
附录 237
附录Ⅰ 国际相对原子量表 237
附录Ⅱ 不同温度下水的饱和蒸汽压 239
附录Ⅲ 常用弱酸弱碱的解离平衡常数 240
附录Ⅳ 化学相关网站 242
附录Ⅴ 参考书目 243
附录Ⅵ 中英文关键词汇表 244