第1篇 质谱分析的研究与应用 3
1-1 Reaction Mass Spectrometry 3
1-2 Stereochemical Effects in Mass Spectrometry 2-Chemical Ionization Mass Spectra of Some Cyclic Glycols and Mono-and Di-saccharides Using Trimethyl Borate as Reagent Gas 19
1-3 Stereochemical Effects in Mass Spectrometry 3 Detection of Chirality by Che-mical Ionization Mass Spectrometry 27
1-4 Stereochemical Studies on Steroids by Mass Spectrometry(Ⅳ)：-Application of Me3SiNEt2 as a Reagent 33
1-5 Stereochemical Effects in Mass Spectra-Studies on Mass Spectra of Epimers of Podophyllotoxin and Its Derivatives 36
1-6 Stereochemical Effects in Mass Spectrometry 43
1-7 Mass Spectrometry of Natural Products Stereochemical Studies by Reaction Mass Spectrometry 49
1-8 CI Mass Spectra of Substituted Phenols with Acetone as Reagent 52
1-9 Stereochemical Effects in Mass Spectrometry：Part 8—Chemical Ionization Mass Spectra of Cyclic Glycols and Monosaccharides Using Formaldehyde Dimethyl Acetal as Reagent Gas 54
1-10 Stereochemical Effects in Mass Spectrometry Part 10 Reaction Mass Spectrometry of Cyclic Glycols and Monosaccharides with Methylene Chloride as Reagent Gas 61
1-11 反应质谱法——超微量立体化学分析新技术 67
1-12 天然有机化合物 77
1-13 Stereochemical Effects in Mass Spectrometry ⅩⅢ Determination of Absolute Configuration by Fast Atom Bombardment Mass Spectrometry 82
1-14 Stereochemical Effects in Mass Spectrometry ⅩⅤ Chemical Ionization of Some Substituted Alkenes Using Dichlorocarbene as the Reagent Gas 90
1-15 Association of the Acylium Ion of Acids with Alcohols as an Esterification Mechanism in Chemical Ionization 95
1-16 Stereochemical Effects in Mass Spectrometry-Determination of the Optical Purity of Enantiomers by Mass Spectrometry 97
1-17 快原子轰击和碰撞活化质谱法研究三萜皂苷结构 102
1-18 Fast Atom Bombardment and Collisional Activation Mass Spectrometry in the Structural Analysis of Steroidal Oligoglycosides 106
1-19 Studies on the mass spectrometry of natural products 115
1-20 天然有机化合物质谱研究 121
1-21 寡糖快原子轰击质谱中碱金属加合离子应用技术的研究 130
1-22 Mass Spectrometry of Oligosaccharides(Ⅰ)-Formation of theM+NH4］+ Ion of Oligosaccharides in Fast Atom Bombardment Mass spectrometry 133
第2篇 天然产物化学 139
2-1 当归化学成分分析研究——毛细管气相色谱-质谱法鉴定当归根挥发油成分 139
2-2 Analysis of Chemical Ingredients of Angelica Sinensis——Analysis of Non-Volatile Constituents of Roots 144
2-3 细花雪胆中的新成分——新葫芦素 152
2-4 Determination of Volatile Constituents of Chinese Medicinal Herbs by Direct Vaporization Capillary Gas Chromatography/Mass Spectrometry 156
2-5 Diterpenoid Alkaloids of Aconitum Sungpanense 167
2-6 Diterpenoids From Rabdosia Henryi 173
2-7 Ganschisandrine，A Lignan from Schisandra Sphenanthera 178
2-8 Diterpenoids from RabdosiaJaponica Var.Glaucocalyx 181
2-9 Diterpenoid Alkaloids from Delphinium Winklerianum 185
2-10 A Diterpenoid Alkaloid from Aconitum Vilmorinianum Var.Patentipilum 191
2-11 Bioactive Sesquiterpene Polyol Esters from Euonymus Bungeanus 195
2-12 Diterpenoids from Rabdosia Pseudo-Irrorata 202
2-13 Diterpenoid Alkaloids from Aconitum Vilmorrianum 208
2-14 Sesquiterpene Polyol Esters from Celastrus Paniculatus 213
2-15 Dihydroagarofuran Sesquiterpenoids from Celastrus Panicula Tus 218
2-16 Diterpenoids from Rabdosia ParVifolia 224
2-17 Diterpenoid Alkaloids from Delphinium caeruleum 229
2-18 Triterpenoid Saponins from Anemone Hupehensis 234
2-19 Diterpenoid Alkaloids from Aconitum Talassicum 240
2-20 Oligostilbenes from Vitis Heyneana 247
2-21 Diterpenoid Alkaloids from Delphinium Caeruleum 252
2-22 Triterpenoid Saponins from Anemone Hupehensis 256
2-23 Diterpenoids from Isodon Gesneroides 261
2-24 TwoNewSesquiterpenes from CelastrusAngulatus 268
2-25 Souline C and Souline D，New Diterpenoid Alkaloids From Delphinium Souliei 272
2-26 A Simplified and Practical Method for Methylation Analysis of Polysaccharides 275
2-27 红芪多糖RHG的分离纯化及化学结构 278
2-28 Diterpenoids from Isodon Leucophyllus 282
2-29 Diterpenoids from Isodon Eriocalyx 288
2-30 Phenylpropanoid Glycosides from LamiophlomisRotata 294
2-31 滇姜花抗肿瘤活性二萜及其光敏氧化反应的研究 299
2-32 ent-Kaurene diterpenoids from Isodon Rubescens 303
2-33 Two Glycosides from the Stem Bark of Tetracentron sinense 309
2-34 Two New Diterpenoids from Isodon Rubescens 314
2-35 卵叶银莲花全草中的新三萜皂苷 316
第3篇 有机分析 325
3-1 Microidentification of Aldehydes andAnines 325
3-2 Two New Solvents for the Rast Method of Microdetermination of Molecular Weights 332
3-3 原子吸收光度法测定还原糖和脂肪仲胺 334
3-4 Study on Spin Labeling Analysis Synthesis and ESR Determination of Spin-Labeled Anti-Tumour Podophyllotoxin Derivatives 337
3-5 Two-dimensional NMR Study of Ganwuweizic Acid 340
3-6 Separation of Polycyclic Aromatic Hydrocarbons by Micellar E1ectrokinetic Chromatography with Aqueous Short-Chain Alcohol Solvent 346
3-7 Chiral Gas Chromatographic Assay with Flame Ionization Detection for Amphetamine Enantiomers in Microsomal Incubates 353
3-8 Carboxymethyl-β-Cyclodextrin for Chiral Separation of Basic Drugs by Capillary Electrophoresis 359
第4篇 有机化学 369
4-1 苯甲酰异硫氰用作鉴定醇类的试剂 369
4-2 磺胺苯并噻唑Ⅳ.具有羧基的磺胺苯并噻唑 371
4-3 甲基硅烷的气相氯化 377
4-4 Acylthiosemicarbazides and Related Compounds 382
4-5 The Total Synthesis of Taxamairin B 386
4-6 The First Total Synthesis of(±)-Demethyl Salvicanol 392
4-7 A Facial One-step Approach to Stereospecific Spirocyclic Diols from α-Hydroxy-epoxides 400
4-8 新的烯丙型环氧醇重排还原反应研究 403
4-9 An Efficient Synthesis of N-Trifluoroacetyl Adriamycin-14-Valerate(AD-32) 407
4-10 Synthesis of Heterocyclic Compounds from 2-Phenyl-1，2，3-Triazole-4-Formy-lhydrazine 410
第5篇 药物化学 419
5-1 Spin-Labeled Antitumor Derivatives of Podophy llotoxin 419
5-2 Anticancer Drugs Ⅱ.Synthesis and Biological Evaluation of Spin Labeled Deriv-atives of Podophyllotoxin 429
5-3 Anticancer Drugs Part Ⅲ：New Spin Labelled Derivatives of Podophyllotoxin 435
5-4 Synthesis and Antitumor Activity of Spin-Labeled Derivatives of Podophyllotoxin 439
5-5 Studies on Spin-Labelled Peptide Nucleic Acid 445
5-6 杂环化合物取代的5-氟尿嘧啶衍生物的合成及抗肿瘤活性 450
5-7 A Facile and Efficient Synthesis of 4β-Aminopodophyllotoxins 453
5-8 Synthesis of Novel 4β-(1，2，3-Triazol-1-y1)Podophyllotoxins as Potential Anti-tumor Drugs 457
5-9 Synthesis of Spin Labeled Carbocyclic Lignan Analogue Related to Podophyllo-toxin 461
5-10 The Synthesis of 6-Alkyl-5-Fluorouracil Derivatives 465
5-11 A Facile and Highly Stereoselective Reductive Debromination of Anhydro-6-(R)-Hydroxyethyl-6-Bromopenicillin 468
5-12 Synthesis of Novel Spin Labeled Analogues of N-(Trifluoroacetyl)-Daunorubicin 470
5-13 Synthesis of 1-Arylated Derivatives of 5-Fluorouracil As Potential Antitumor Drug 474
5-14 4β-氨基-4-脱氧鬼臼毒素和4β-氨基-4-脱氧-4′-去甲基鬼臼毒素的两种新合成方法 477