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Four New Coordination Polymers of Cu(Ⅱ)with 1,1′-(1,4-butanediyl)Bis(Imidazole) 1

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Synthesis and Characterization of β-diketonato Titanium Derivatives of Polyoxometalates 18

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Synthesis and Antitumor Activity of Cyclopentadienyltitanium Substituted Polyoxotungstate[oW11O39(CpTi)]7-(Cp=η5-C5H5) 26

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A Porous Supramolecular Architecture from a Copper(Ⅱ)Coordination Polymer with a 3D Four-connected 86 Net 38

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New Polyoxometalate-starch Nanomaterial:Synthesis Characterization and Antitumoral Activity 48

Synthesis,Spectroscopic Characterization and Antitumor Activityin vitro of Organometallo Substituted Polyoxotungstates(RM)3 P2W15O59n-(RM=CpTi,CpZr,C4H7O2Sn or C5H9O2Sn) 58

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The First Ladder Structure Containing Three Different Squares:The Structure of Barium 3-carboxy-4-hydroxybenzenesulfonate 65

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Comparison of Catalytical and Biological Activities for Substituted Polyoxotungstates Containing Ti and CpTi 72

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Synthesis and Spectroscopic Characterization of Organophosphoryl Tungstosilicates α-[RP(O)]2SiW11O394- 81

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Synthesis and Crystal Structure of the Dimeric Ti—O—Ti Bridged Hydrid Form Polyoxoanion[α-1,2-PW10Ti2O39]210- 86

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Synthesis,183W NMR Spectroscopic Characterization and Properties of Trisubstituted Heteropolytungstates Containing Group 3A Elements 94

Synthesis,Characterization and In Vitro Antitumor Activity of Diorganometallo Complexes γ-Keggin Anions 104

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1H NMR Study of Pyridine-type Ligands Coordinated to the Paramagnetic Polyoxometalates,[CoⅡW11MO39]n-(M=CoⅡ,NiⅡ,CuⅡ,or FeⅢ) 109

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Synthesis and Characterization of Organotin Substituted Heteropolytungstophosphates and Their Biological Activity 124

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Effect of Glucose-lowering of Heteropolytungstogermanate β-K6H[GeW9V3O40]·9H2O 135

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Synthesis and Characterization of Organophosphoryl Polyoxotungstate[α2-R2P2W17O61]6-(R=C6H11P(O),C6H5P(O),C6H11P(S),C6H5P(S)) 142

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Synthesis and Spectroscopic Characterization of Organophosphoryl Polyoxotungstates[C6H11P(O)]2Xn+W11O39(8-n)-(Xn+=P5+,Si4+,B3+,Ga3+) 147

Two New Coordination Polymers of Co(Ⅱ)with 1,1′-(1,4-butanediyl)Bis(Benzimidazole) 156

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Networks with Hexagonal Circuits in Co-ordination Polymers of Metal Ions(ZnⅡ,CdⅡ)with 1,1′-(1,4-butanediyl)Bis(Imidazole) 166

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三苯基锡—2—（1,2—亚乙二硫）亚甲基—3—羰基—5—芳基—4—戊烯酸酯的合成及晶体结构 181

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Synthesis,Characterization and Biological Activity of Organotitanium Substituted Heteropolytungstates 193

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An Unusual Electrochemically Induced Demetalation of Iron-substituted Keggin-type Undecatungstozincate ZnW11FeⅢ(H2O)O397- 202

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Electrochemical Behavior of a Series of UndecatungstozincatesMonosubstituted by First-row Transition Metals,ZnW11 M(H2O)O39n-(M=Cr,Mn,Fe,Co,Ni,Cu or Zn) 210

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Redox Electrochemistry of Silicon Dioxide Gel Films Containing 1∶12 Molybdosilicate Acid and Its Electrocatalytic Activity toward the Reduction of Nitrite Ions 228

夹心杂多化合物的合成及晶体结构 241

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Synthesis and Characterization of Organotin-substituted Heteropoly Tungstosilicates and Their Biological Activity I 250

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Synthesis,Properties and Crystal Structure of the Charge-transfer Salt(DBTTF)6 HSiMo12O404H2O 265

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Electrochemical and Electrocatalytic Properties of Tetra-iron Substituted Sandwich-type Pentadecatungstodiphosphate Heteropolyanions 274

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含钒（Ⅳ）和钒（Ⅴ）的钨锗混合价杂多酸盐的合成及其结构表征 283

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Synthesis and 183W and 51V NMR Characterization of α-and β-K6 H[GeW9V3O40]·xH2O and ESR Spectra of Mixed-valence Vanadium Polyanions 290

镧系元素的双—（9—钨—2—钼磷）杂多酸钾的合成与性质研究 298

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α—B—Keggin型杂多化合物K5H[Co4(VW9O33)2]·5H2O的合成和结构 302

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Synthesis and Characterization of Novel Heteropoly-tungstoarsenates Containing Lanthanides[LnAs4W40O140]25-and Their Biological Activity 310

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Synthesis,Structure and Properties of Undecatungstozincate Containing 3A Elements 320

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Synthesis,Properties and Crystal Structure of a Heteropoly Compound Containing Titanium 329

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Synthesis and Properties of Undecatungstozincates with a Transition Metal 337

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Heteropoly Complexes Containing Titanium—I.The Complexes with Tetrahedral Iron or Chromium as Central Atom 349

Synthesis and Characterization ofα,β-triindium Substituted Heteropolytungstates 357

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α—和β—［SiW9Ti3O40]10-的合成及其钨—183核磁共振表征 365

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Synthesis and Characterization of Bis(Undecatungstoarsenate)Lanthanates of Potassium 371

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Synthesis and Characterization of Bis(Undecatungstocuprate)Lanthanates of Potassium 380

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Derivatives of the 21-tungsto-9-antimonate Heteropolyanion.Part 1.Inclusion of Lanthanide Cations 390

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Trimetallo Derivatives of Lacunary 9-Tungstosilicate Heteropolyanions.Part 1.Synthesis and Characterization 397

Synthesis and Characterization of Undecatungstotitanates Incorporating a Lanthanide or A Transition Metal 414

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Emission Spectra of Some Heteropolytungstates Containing Europium 423

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Synthesis and Characterization of Bis(Undecatungstoferrate)Lanthanates of Potassium 430

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Synthesis and Characterization of Bis(Undecatungstogallate) Lanthanates of Potassium 440

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镧系元素的双（十七钨二砷）杂多酸钾的合成和鉴定 450

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Bis(undecatungstogermanate)Lanthanates of Potassium 461

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镧系元素杂多钨砷酸盐的合成与性质研究 470