应用化学实验 双语版PDF电子书下载

实验1 植物叶绿体色素的提取、分离和鉴定 1

实验2 阿司匹林的合成、鉴定与含量的测定 6

实验3 对氨基苯甲酸乙酯的多步骤合成 9

实验4 苯妥英钠的合成 11

实验5 1,2－二苯基乙二胺外消旋体的拆分 14

实验6 相转移催化合成外消旋扁桃酸及其拆分 17

实验7 pH敏感高分子的合成与相分离临界pH值的测定 20

实验8 二氧化硅／聚甲基丙烯酸甲酯核／壳复合微球的制备及表征 24

实验9 聚苯胺的制备及表征 28

实验10 金属模板法制备四苯基卟啉铜 31

实验11 2－硝基四苯基卟啉铜的合成、表征和性能测定 33

实验12 二茂铁及其衍生物的合成与纯化 35

实验13 三价钴配位化合物的合成及红外光谱表征 38

实验14 铁的草酸盐配合物的制备、分析与性质 40

实验15 纳米TiO2的制备及光催化性能 43

实验16 多壁碳纳米管的对氨基苯磺酸钠修饰及对Cu2+的吸附性能 45

附录1 常见基团和化学键的红外特征吸收频率 48

附录2 常用有机溶剂的物理常数 49

附录3 常用pH标准缓冲溶液 50

Experiment 1 Extraction,separation and characterization of chloroplast pigments 54

Experiment 2 Synthesis,characterization and content determination of aspirin 60

Experiment 3 Preparation of ethyl p-aminobenzoate 64

Experiment 4 Synthesis of phenytoin sodium 67

Experiment 5 Resolution of 1,2-diphenylethylenediamine 70

Experiment 6 Synthesis of mandelic acid by phase transfer catalysis and its resolution 75

Experiment 7 Synthesis of pH-sensitive polymer and the determination of the critical pH for phase separation 79

Experiment 8 Synthesis and characterization of core-shell SiO2-PMMA composite microsphere 84

Experiment 9 Preparation and characterization of polyaniline 88

Experiment 10 Preparation of copper tetraphenylporphyrin by metal formwork 92

Experiment 11 Synthesis,characterization and performance of 2-nitro-tetraphenylporphyrin 95

Experiment 12 Synthesis of ferrocene and its derivants 98

Experiment 13 Synthesis and characterization of trivalent cobalt complexes 103

Experiment 14 Preparation,analysis and characteristic of the complex of iron and oxalate 106

Experiment 15 Preparation of nano-TiO2 and its photocatalytic activity 109

Experiment 16 Modification of carbon nanotubes with sodium p-aminobenzenesulfonate and its absorption on Cu2+ 112

Appendiex 1 The IR absorption frequencies of normal groups and chemical bonds 115

Appendiex 2 Physical properties of common solvents 116

Appendiex 3 Preparation of pH buffer solutions 117